(a) Soundness Test: It is
conducted by sieve analysis. 100 gms of cement is taken and sieved
through IS sieve No. 9 for fifteen minutes. Residue on the sieve is
weighed. This should not exceed 10 per cent by weight of sample
taken.
(b) Setting Time: Initial
setting time and final setting time are the two important physical
properties of cement. Initial setting time is the time taken by the
cement from adding of water to the starting of losing its plasticity.
Final setting time is the time lapsed from adding of the water to
complete loss of plasticity. Vicat apparatus is used for finding the
setting times [Ref. Fig. 1.5].
FIG 1.5 – PARTS OF VICAT APPARATUS
Vicat apparatus consists of a movable
rod to which any one of the three needles shown in figure can be
attached. An indicator is attached to the movable rod. A vicat mould
is associated with this apparatus which is in the form of split
cylinder.
Before finding initial and final
setting time it is necessary to determine water to be added to get
standard consistency. For this 300 gms of cement is mixed with about
30% water and cement paste prepared is filled in the mould which
rests on non porous plate. The plunger is attached to the movable rod
of vicat apparatus and gently lowered to touch the paste in the
mould. Then the plunger is allowed to move freely.
If the penetration is 5 mm to 7 mm from
the bottom of the mould, then cement is having standard consistency.
If not, experiment is repeated with different proportion of water
fill water required for standard consistency is found. Then the tests
for initial and final setting times can be carried out as explained
below:
Initial Setting Time: 300 gms of cement
is thoroughly mixed with 0.85 times the water for standard
consistency and vicat mould is completely filled and top surface is
levelled. 1 mm square needle is fixed to the rod and gently placed
over the paste. Then it is freely allowed to penetrate.
In the beginning the needle penetrates
the paste completely. As time lapses the paste start losing its
plasticity and offers resistance to penetration. When needle can
penetrate up to 5 to 7 mm above bottom of the paste experiment is
stopped and time lapsed between the addition of water and end if the
\ experiment is noted as initial setting time.
Final Setting Time. The square needle
is replaced with annular collar. Experiment is continued by allowing
this needle to freely move after gently touching the surface of the
paste. Time lapsed between the addition of water and the mark of
needle but not of annular ring is found on the paste. This time is
noted as final setting time.
(c) Soundness Test: This test is
conducted to find free lime in cement, which is not desirable. Le
Chatelier apparatus is used for conducting this test. It consists of
a split brass mould of diameter 30 mm and height 30 mm. On either
side of the split, there are two indicators, with pointed ends.
The ends of indicators are 165 mm from
the centre of the mould. another glass plate and a small weight is
placed over it. Then the whole assembly is kept under water for 24
hours. The temperature of water should be between 24°C and 50°C.
Note the distance between the
indicator. Then place the mould again in the water and heat the
assembly such that water reaches the boiling point in 30 minutes.
Boil the water for one hour. The mould is removed from water and
allowed to cool.
The distance between the two pointers
is measured. The difference between the two readings indicate the
expansion of the cement due to the presence of unburnt lime. This
value should not exceed 10 mm.
(d) Crushing Strength Test: For
this 200 gm of cement is mixed with 600 gm of standard sand
confirming to IS 650–1966. After mixing thoroughly in dry condition
for a minute distilled potable water P/4 + 3 percentage is added
where P is the water required for the standard consistency.
They are mixed with trowel for 3 to 4
minutes to get uniform mixture. The mix is placed in a cube mould of
70.6 mm size (Area 5000 mm2) kept on a steel plate and prodded with
25 mm standard steel rod 20 times within 8 seconds.
Then the mould is placed on a standard
vibrating table that vibrates at a speed of 12000 ± 400 vibration
per minute. A hopper is secured at the top and the remaining mortar
is filled. The mould is vibrated for two minutes and hopper removed.
The top is finished with a knife or with a trowel and levelled. After
24 ± 1 hour mould is removed and cube is placed under clean water
for curing.
After specified period cubes are tested
in compression testing machine, keeping the specimen on its level
edges. Average of three cubes is reported as crushing strength. The
compressive strength at the end of 3 days should not be less than
11.5 N/mm2 and that at the end of 7 days not less than 17.5 N/mm2.




